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Beilstein J. Org. Chem. 2014, 10, 1308–1316, doi:10.3762/bjoc.10.132
Graphical Abstract
Scheme 1: Synthesis of macrocycles 3 and 4.
Figure 1: 1H NMR spectra of macrocycles 3a–d, with key proton resonances for the spacing units and key benzyl...
Figure 2: 1H NMR spectroscopy of macrocycles 4a–d, with proton resonances for the spacing units and key benzy...
Figure 3: CD spectra of macrocycles 3b, 3d, 4b, 4d in EtOH (0.5–12 × 10−6 M).
Figure 4: UV–vis titration of C60 (1.8 × 10−4 M) in toluene with increasing amounts of macrocycle 4b (top) an...